Title: Additive Manufacturing of High Temperature Ceramic Heat Exchanger
Authors: Nancy Zheng, Jayanta Deb, Jihua Gou
DOI: 10.33599/nasampe/c.25.213
Abstract: With increasing space exploration over recent years, there is growing interest in the reusability of launch vehicles. Re-entry vehicles experience ablation on the surface due to aerothermal heating imposed on them during the atmospheric entry, and the temperatures at the leading edge can be as high as above 2000 °C. These vehicles required a heat regulator to ensure the surface temperatures are within operating tolerances and reduce the maintenance needs upon return. Ceramics are known for its stable properties and high heat resistivity and the primary material selected is a commercial alumina resin. The heat exchanger proposed forms a honeycomb structure of consecutive matrix panels aligning to one another in a stairway pattern. Due to the complexity and capability of scaling, the structure was additively printed through polymerization of the ceramic resin utilizing digital light processing (DLP) and then undergoing polymerization to form the final structure. The part was sintered at 1510 °C in a single firing schedule spanning approximately 86 hours. It was measured that there is a horizontal shrinkage of around 19 % after furnace treatment and 93% relative density. The study presents the design and geometry of ceramic heat exchanger, shrinkage of the part after pyrolysis, material characterization, and a simulation and analysis of heat transfer and circulation of cooling fluid to maintain temperatures. The simulation study was conducted using COMSOL Multiphysics where the diffusing of heat through the solid ceramic panel and a cooling fluid was introduced.
References: [1] F. Raether. "Ceramic Matrix Composites - an Alternative for Challenging Construction Tasks." Ceramic Applications. Fraunhofer-Center for High Temperature Materials and Design HTL (1): 45–49. 2013. [2] Callister, W Jr, Rethwisch, D. Fundamentals of Materials Science and Engineering: An Integrated Approach. 4st ed. John Wiley & Sons, Inc. Hoboken. NJ, 2012. [3] Liu, L., Li, X., Xing, X., Zhou, C., & Hu, H. A modified polymethylsilane as the precursor for ceramic matrix composites. China: Journal of Organometallic Chemistry, 693(6), 917922. 2008. [4] Cao, F., Li, X. D., & Kim, D. P. Efficient curing of polymethylsilane by borazine and reaction mechanism study. China: Journal of Organometallic Chemistry, 688(1–2), 125–131. 2003. [5] Sreeja, R., Swaminathan, B., Painuly, A., Sebastian, T. V., & Packirisamy, S. Allylhydridopolycarbosilane (AhPCS) as matrix resin for C-SiC ceramic matrix composites. Materials Science and Engineering, 168(1-3), 204-207. 2010. [6] Yu, Z., Huang, M., Fang, Y., Li, R., Zhan, J., Zeng, B., … Zhang, L. Modification of a liquid polycarbosilane with 9-BBN as a high-ceramic-yield precursor for SiC. Reactive and Functional Polymers, 70(6), 334–339. 2010. [7] Starfire System. SPR688 Data sheet. 2017.12 [8] Starfire System. SMP10 Data sheet. 2017.13 [9] Jian, K., Chen, Z. H., Ma, Q. S., Hu, H. feng, & Zheng, W. W. Effects of polycarbosilane infiltration processes on the microstructure and mechanical properties of 3D-Cf/SiC composites. 2007. [10] Jian, K., Chen, Z. H., Ma, Q. S., Hu, H. feng, & Zheng, W. W. Effects of pyrolysis temperatures on the microstructure and mechanical properties of 2D-Cf/SiC composites using polycarbosilane. 2007. [11] Jian, K., Chen, Z. H., Ma, Q. S., & Zheng, W. W. Effects of pyrolysis processes on the microstructures and mechanical properties of Cf/SiC composites using polycarbosilane. 2005. [12] Chai, Y., Zhang, H., Zhou, X., & Yang, B. Effect of pyrolysis temperatures on the performance of SiCf/SiC composites. Fusion Engineering and Design, 125, 447–453. 2007. [13] Standard Test Method for Flexural Properties of Continuous Fiber-Reinforced Advanced Ceramic Composites. ASTM C1341-13, 2018. [14] Standard Test Method for Oxyacetylene Ablation Testing of Thermal Insulation Materials. ASTM E285-08, 2020. [15] Standard Test Method for Flexural Properties of Continuous Fiber-Reinforced Advanced Ceramic Composites. ASTM C1341-13, 2018. [16] A. Paul, J. G. P. Binner, B. Vaidhyanathan, A. C. J. Heaton & P. M. Brown. Heat flux mapping of oxyacetylene flames and their use to characterize Cf-HfB2 composites, Advances in Applied Ceramics, 2016. [17] Dae-Hyun Cho, Jin-Seon Kima, Sang-Hyuk Kwona, Changgu Lee, Young-Ze Lee. Evaluation of hexagonal boron nitride nano-sheets as a lubricant additive in water, Wear, Volume 302, Issues 1–2, April–May 2013. [18] J.M. Martin, N. Ohmae. Nanolubricants, (second ed.), John Wiley & Sons, New York, 2008. [19] Issam Elwan, Rafi Jabra, Mohamed Hamzeh Arafeh. Preparation and Ablation Performance of Lightweight Phenolic Composite Material under Oxyacetylene Torch Environment, Journal of Aerospace Technology and Management, 2018.
Conference: CAMX 2025
Publication Date: 2025/09/08
SKU: 213
Pages: 15
Price: $30.00
Get This Paper